Structural characterisation of neutrophil glycans by ultra sensitive mass spectrometric glycomics methodology
نویسندگان
چکیده
منابع مشابه
Solid-phase permethylation of glycans for mass spectrometric analysis.
A miniaturized approach was developed for quantitative permethylation of oligosaccharides, which involves packing of sodium hydroxide powder in microspin columns or fused-silica capillaries (500 microm i.d.), permitting effective derivatization in less than a minute at microscale. Prior to mass spectrometry, analytes are mixed with methyl iodide in dimethyl sulfoxide solution containing traces ...
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ژورنال
عنوان ژورنال: Glycoconjugate Journal
سال: 2008
ISSN: 0282-0080,1573-4986
DOI: 10.1007/s10719-008-9146-4